{"id":1119,"date":"2022-05-02T14:46:40","date_gmt":"2022-05-02T14:46:40","guid":{"rendered":"https:\/\/phynd.polimi.it\/?page_id=1119"},"modified":"2023-05-29T08:05:44","modified_gmt":"2023-05-29T08:05:44","slug":"equipment","status":"publish","type":"page","link":"https:\/\/phynd.polimi.it\/?page_id=1119","title":{"rendered":"Equipment and Methods"},"content":{"rendered":"\n<p class=\"wp-block-paragraph\">Our activities involve a range of techniques for the <a href=\"#EquGro\" data-type=\"internal\" data-id=\"#EquGro\">growth <\/a>of thin films and heterostructures, the nanoscale and bulk <a href=\"#EquCha\" data-type=\"internal\" data-id=\"#EquCha\">characterization<\/a>, the <a href=\"#EquNan\">nanofabrication<\/a> and <a href=\"#EquMod\" data-type=\"internal\" data-id=\"#EquMod\">simulations<\/a>.<\/p>\n\n\n\n<h3 class=\"wp-block-heading has-text-align-center\" id=\"EquNan\"><br>Advanced Nanofabrication<\/h3>\n\n\n\n<h4 class=\"wp-block-heading\">Thermal Scanning Probe Lithography (tSPL) + Laser Writing &#8211; NanoFrazor Explore <\/h4>\n\n\n\n<div class=\"wp-block-media-text alignwide is-stacked-on-mobile\" style=\"grid-template-columns:25% auto\"><figure class=\"wp-block-media-text__media\"><img loading=\"lazy\" decoding=\"async\" width=\"852\" height=\"639\" src=\"https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/NFE_inside_smaller.jpg\" alt=\"\" class=\"wp-image-1144 size-thumbnail\" srcset=\"https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/NFE_inside_smaller.jpg 852w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/NFE_inside_smaller-300x225.jpg 300w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/NFE_inside_smaller-768x576.jpg 768w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/NFE_inside_smaller-700x525.jpg 700w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/NFE_inside_smaller-520x390.jpg 520w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/NFE_inside_smaller-360x270.jpg 360w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/NFE_inside_smaller-250x188.jpg 250w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/NFE_inside_smaller-100x75.jpg 100w\" sizes=\"auto, (max-width: 852px) 100vw, 852px\" \/><\/figure><div class=\"wp-block-media-text__content\">\n<p class=\"wp-block-paragraph\">The Heidelberg NanoFrazor Explore is a dedicated Thermal Scanning Probe Lithography nanofabrication tool. It uses a ultra-sharp heatable probe tip for locally heating the substrate with sub-10 resolution. It is also equipped with a laser writer module for allowing mix-and-match tSPL and laser lithography. It allows in-situ imaging, markerless alignment, 3D nanopatterning capabilities with &lt; 1 nm vertical resolution. The NanoFrazor equipped with a tuable magnetic field is used for performing thermally assisted magnetic scanning probe lithography (tam-SPL).<\/p>\n<\/div><\/div>\n\n\n\n<h4 class=\"wp-block-heading\">Thermal Scanning Probe Lithography (tSPL) &#8211; Keysight 5600LS<\/h4>\n\n\n\n<div class=\"wp-block-media-text alignwide is-stacked-on-mobile\" style=\"grid-template-columns:25% auto\"><figure class=\"wp-block-media-text__media\"><img loading=\"lazy\" decoding=\"async\" width=\"1024\" height=\"891\" src=\"https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Senza-titolo-1024x891.png\" alt=\"\" class=\"wp-image-1146 size-thumbnail\" srcset=\"https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Senza-titolo-1024x891.png 1024w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Senza-titolo-300x261.png 300w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Senza-titolo-768x668.png 768w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Senza-titolo-700x609.png 700w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Senza-titolo-520x452.png 520w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Senza-titolo-360x313.png 360w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Senza-titolo-250x217.png 250w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Senza-titolo-100x87.png 100w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Senza-titolo.png 1291w\" sizes=\"auto, (max-width: 1024px) 100vw, 1024px\" \/><\/figure><div class=\"wp-block-media-text__content\">\n<p class=\"wp-block-paragraph\">tSPL and tamSPL are performed also using a customized 5600LS AFM system. The 5600LS AFM allows imaging of both large samples (in air) and small samples (in air, or in liquid under temperature control). The 5600LS utilizes a 200 mm x 200 mm, fully addressable and programmable stage, as well as a low-noise AFM design. Samples up to 8\u201d in diameter and 30mm tall are easily accepted by the 200mm vacuum chuck. The stage accommodates a 300 mm wafer with repositioning.<\/p>\n<\/div><\/div>\n\n\n\n<h4 class=\"wp-block-heading\">Optical \/ E-beam lithography &#8211; PoliFab <\/h4>\n\n\n\n<div class=\"wp-block-media-text alignwide is-stacked-on-mobile\" style=\"grid-template-columns:25% auto\"><figure class=\"wp-block-media-text__media\"><img loading=\"lazy\" decoding=\"async\" width=\"667\" height=\"345\" src=\"https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-220353.png\" alt=\"\" class=\"wp-image-1154 size-thumbnail\" srcset=\"https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-220353.png 667w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-220353-300x155.png 300w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-220353-520x269.png 520w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-220353-360x186.png 360w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-220353-250x129.png 250w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-220353-100x52.png 100w\" sizes=\"auto, (max-width: 667px) 100vw, 667px\" \/><\/figure><div class=\"wp-block-media-text__content\">\n<p class=\"wp-block-paragraph\">Micro-nanofabrication techniques such as equipment for performing Optical \/ EBeam lithography are available in PoliFab, the micro-nanofabrication center of Politecnico di Milano<\/p>\n<\/div><\/div>\n\n\n\n<hr class=\"wp-block-separator has-text-color has-css-opacity has-background is-style-wide\" style=\"background-color:#fc9f00;color:#fc9f00\"\/>\n\n\n\n<h3 class=\"wp-block-heading has-text-align-center\" id=\"EquCha\"><br>Characterization <\/h3>\n\n\n\n<h4 class=\"wp-block-heading\">Scanning Probe Microscopy &#8211; Park NX 10 <\/h4>\n\n\n\n<div class=\"wp-block-media-text alignwide is-stacked-on-mobile\" style=\"grid-template-columns:25% auto\"><figure class=\"wp-block-media-text__media\"><img loading=\"lazy\" decoding=\"async\" width=\"840\" height=\"757\" src=\"https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-172441.png\" alt=\"\" class=\"wp-image-1134 size-thumbnail\" srcset=\"https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-172441.png 840w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-172441-300x270.png 300w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-172441-768x692.png 768w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-172441-700x631.png 700w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-172441-520x469.png 520w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-172441-360x324.png 360w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-172441-250x225.png 250w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-172441-100x90.png 100w\" sizes=\"auto, (max-width: 840px) 100vw, 840px\" \/><\/figure><div class=\"wp-block-media-text__content\">\n<p class=\"wp-block-paragraph\">The Park NX 10 Scanning Probe Microscope allows to characterize with nanoscale resolution the morphology, electrical \/ magnetic properties, nanomechanical and thermal properties of a wide range of systems. A motorized coarse positioning system allows to investigate samples up to 2&#215;2 cm2. The microscope is equipped with an 100&#215;100 um2 in-plane piezoscanner. Measurements mode available include: AFM, Magnetic Force Microscopy in a variable magnetic field, Conductive-AFM, Kelvin Probe Force Microscopy, Piezo-Force Microscopy, Scanning Thermal Microscopy, Nanomechanics. A heatable stage from RT up to 250\u00b0C can be employed.<\/p>\n<\/div><\/div>\n\n\n\n<h4 class=\"wp-block-heading\">Kerr Magnetometry and Kerr Microscopy<\/h4>\n\n\n\n<div class=\"wp-block-media-text alignwide is-stacked-on-mobile\" style=\"grid-template-columns:25% auto\"><figure class=\"wp-block-media-text__media\"><img loading=\"lazy\" decoding=\"async\" width=\"1024\" height=\"852\" src=\"https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/20210517_104643-scaled-1-1024x852.jpg\" alt=\"\" class=\"wp-image-1137 size-thumbnail\" srcset=\"https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/20210517_104643-scaled-1-1024x852.jpg 1024w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/20210517_104643-scaled-1-300x250.jpg 300w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/20210517_104643-scaled-1-768x639.jpg 768w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/20210517_104643-scaled-1-1536x1278.jpg 1536w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/20210517_104643-scaled-1-2048x1704.jpg 2048w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/20210517_104643-scaled-1-700x582.jpg 700w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/20210517_104643-scaled-1-520x433.jpg 520w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/20210517_104643-scaled-1-360x300.jpg 360w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/20210517_104643-scaled-1-250x208.jpg 250w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/20210517_104643-scaled-1-100x83.jpg 100w\" sizes=\"auto, (max-width: 1024px) 100vw, 1024px\" \/><\/figure><div class=\"wp-block-media-text__content\">\n<p class=\"wp-block-paragraph\">The Magneto-Optical Kerr Effect (MOKE) provides a powerful way for studying the magnetic behaviour of thin films by simply analyzing the light reflected from their surface. The incident light is polarized linearly before reaching the sample; the reflected light is analyzed through a polarizer (the analyzer). Two different setups are used depending on the application:<\/p>\n\n\n\n<ul class=\"wp-block-list\">\n<li>The table-top MOKE setup uses laser light from a 532 nm diode, focused on the sample surface. The longitudinal or polar configuration give access to the in-plane or out-of-plane component of the magnetization with respect to the sample surface, as a function of the external magnetic field.<\/li>\n\n\n\n<li>The MOKE Microscope allows to acquire images with magnetic contrast, as a function of the external magnetic field. It uses Kohler illumination via a high intensity LED lamp.<\/li>\n<\/ul>\n<\/div><\/div>\n\n\n\n<h4 class=\"wp-block-heading\">Vibrating Sample Magnetometry (VSM)<\/h4>\n\n\n\n<div class=\"wp-block-media-text alignwide is-stacked-on-mobile\" style=\"grid-template-columns:25% auto\"><figure class=\"wp-block-media-text__media\"><img loading=\"lazy\" decoding=\"async\" width=\"330\" height=\"300\" src=\"https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/TESI21spec_Girardi_Towards-three-dimensional-imaging-of-spin-waves.jpg\" alt=\"\" class=\"wp-image-1142 size-thumbnail\" srcset=\"https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/TESI21spec_Girardi_Towards-three-dimensional-imaging-of-spin-waves.jpg 330w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/TESI21spec_Girardi_Towards-three-dimensional-imaging-of-spin-waves-300x273.jpg 300w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/TESI21spec_Girardi_Towards-three-dimensional-imaging-of-spin-waves-250x227.jpg 250w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/TESI21spec_Girardi_Towards-three-dimensional-imaging-of-spin-waves-100x91.jpg 100w\" sizes=\"auto, (max-width: 330px) 100vw, 330px\" \/><\/figure><div class=\"wp-block-media-text__content\">\n<p class=\"wp-block-paragraph\">The Microsense, LLC. Easy VSM model EZ-9A allows to measure quantitatively the magnetic properties of the samples. A maximum field of 2.25 T can be applied, and it can measure magnetic moments down to \u03bcemu. It allows a fully automated rotation of the sample of 360\u00b0 and it is possible to support operations with a temperature ranging from 100 K to 1000 K and a temperature rate up to 60-100 K\/min.<\/p>\n<\/div><\/div>\n\n\n\n<h4 class=\"wp-block-heading\">Electronic transport measurements<\/h4>\n\n\n\n<div class=\"wp-block-media-text alignwide is-stacked-on-mobile\" style=\"grid-template-columns:25% auto\"><figure class=\"wp-block-media-text__media\"><img loading=\"lazy\" decoding=\"async\" width=\"442\" height=\"338\" src=\"https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-233656.png\" alt=\"\" class=\"wp-image-1178 size-thumbnail\" srcset=\"https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-233656.png 442w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-233656-300x229.png 300w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-233656-360x275.png 360w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-233656-250x191.png 250w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-233656-100x76.png 100w\" sizes=\"auto, (max-width: 442px) 100vw, 442px\" \/><\/figure><div class=\"wp-block-media-text__content\">\n<p class=\"wp-block-paragraph\">Transport measurements are performed either via probes or wire bonding using different setups. Measurements include I-V curves, magnetoresistance, Hall effect. <\/p>\n\n\n\n<ul class=\"wp-block-list\">\n<li>Table top 4-point or 2-point probe measurements for room temperature measurements as a function of the external magnetic field.<\/li>\n\n\n\n<li>Electrical measurements in the temperature range 10 K-450 K are performed using a closed circuit He cryostat (Displex CS-202NE from ARS).<\/li>\n<\/ul>\n<\/div><\/div>\n\n\n\n<hr class=\"wp-block-separator has-text-color has-css-opacity has-background is-style-wide\" style=\"background-color:#fc9f00;color:#fc9f00\"\/>\n\n\n\n<h3 class=\"wp-block-heading has-text-align-center\" id=\"EquGro\"><br>Growth of thin films<\/h3>\n\n\n\n<h4 class=\"wp-block-heading\">Magnetron Sputtering &#8211; AJA ATC Orion 8  <\/h4>\n\n\n\n<div class=\"wp-block-media-text alignwide is-stacked-on-mobile\" style=\"grid-template-columns:25% auto\"><figure class=\"wp-block-media-text__media\"><img loading=\"lazy\" decoding=\"async\" width=\"800\" height=\"696\" src=\"https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/AJA-ATC-Orion-8-.jpg\" alt=\"\" class=\"wp-image-1128 size-thumbnail\" srcset=\"https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/AJA-ATC-Orion-8-.jpg 800w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/AJA-ATC-Orion-8--300x261.jpg 300w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/AJA-ATC-Orion-8--768x668.jpg 768w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/AJA-ATC-Orion-8--700x609.jpg 700w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/AJA-ATC-Orion-8--520x452.jpg 520w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/AJA-ATC-Orion-8--360x313.jpg 360w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/AJA-ATC-Orion-8--250x218.jpg 250w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/AJA-ATC-Orion-8--100x87.jpg 100w\" sizes=\"auto, (max-width: 800px) 100vw, 800px\" \/><\/figure><div class=\"wp-block-media-text__content\">\n<p class=\"wp-block-paragraph\">Equipment for deposition of thin films using magnetron sputtering on 3\u201d substrates. Typical use: growth of magnetic heterostructures and dielectric materials deposition. The AJA system is provided with ten 2\u201d\/1\u201d, DC and\/or RF, magnetron sputtering sources, which are arranged in a confocal, sputtering-up configuration. The system allows to deposit multilayer structures with precise and automatic control of film thickness.<\/p>\n<\/div><\/div>\n\n\n\n<hr class=\"wp-block-separator has-text-color has-css-opacity has-background is-style-wide\" style=\"background-color:#fc9f00;color:#fc9f00\"\/>\n\n\n\n<h3 class=\"wp-block-heading has-text-align-center\" id=\"EquMod\"><br>Modelling and Simulations<\/h3>\n\n\n\n<h4 class=\"wp-block-heading\">Workstation<\/h4>\n\n\n\n<div class=\"wp-block-media-text alignwide is-stacked-on-mobile\" style=\"grid-template-columns:25% auto\"><figure class=\"wp-block-media-text__media\"><img loading=\"lazy\" decoding=\"async\" width=\"250\" height=\"243\" src=\"https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-221441.png\" alt=\"\" class=\"wp-image-1156 size-thumbnail\" srcset=\"https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-221441.png 250w, https:\/\/phynd.polimi.it\/wp-content\/uploads\/2022\/05\/Immagine-2022-05-02-221441-100x97.png 100w\" sizes=\"auto, (max-width: 250px) 100vw, 250px\" \/><\/figure><div class=\"wp-block-media-text__content\">\n<p class=\"wp-block-paragraph\">A dedicated Workstation equipped with a GeForce RTX 3080 Ti GPU, an Intel Core i9-12900K CPU and 128 GB RAM is used for performing finite element simulations and other labor-intensive tasks. Examples are MuMax3\/OOMMF for performing micromagnetic simulations or COMSOL.<\/p>\n<\/div><\/div>\n\n\n\n<p class=\"has-text-align-left wp-block-paragraph\"><br><br><a href=\"#EquNan\">Go Up<\/a><\/p>\n","protected":false},"excerpt":{"rendered":"<p>Our activities involve a range of techniques for the growth of thin films and heterostructures, the nanoscale and bulk characterization, the nanofabrication [&hellip;]<\/p>\n","protected":false},"author":3,"featured_media":0,"parent":0,"menu_order":0,"comment_status":"closed","ping_status":"closed","template":"page-templates\/page_fullwidth.php","meta":{"_crdt_document":"","footnotes":""},"class_list":["post-1119","page","type-page","status-publish","hentry"],"_links":{"self":[{"href":"https:\/\/phynd.polimi.it\/index.php?rest_route=\/wp\/v2\/pages\/1119","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/phynd.polimi.it\/index.php?rest_route=\/wp\/v2\/pages"}],"about":[{"href":"https:\/\/phynd.polimi.it\/index.php?rest_route=\/wp\/v2\/types\/page"}],"author":[{"embeddable":true,"href":"https:\/\/phynd.polimi.it\/index.php?rest_route=\/wp\/v2\/users\/3"}],"replies":[{"embeddable":true,"href":"https:\/\/phynd.polimi.it\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=1119"}],"version-history":[{"count":44,"href":"https:\/\/phynd.polimi.it\/index.php?rest_route=\/wp\/v2\/pages\/1119\/revisions"}],"predecessor-version":[{"id":1431,"href":"https:\/\/phynd.polimi.it\/index.php?rest_route=\/wp\/v2\/pages\/1119\/revisions\/1431"}],"wp:attachment":[{"href":"https:\/\/phynd.polimi.it\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=1119"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}